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Nanometer-sized YPO4:Eu and YVO4:Eu particles were prepared from alkaline alcohol-water mixture with Y(NO3)3 6H2O, EuCl3 and H3PO4 (or NH4VO4) under reflux. The resultant particles were well crystallized ranging 10-50 nm in diameter by changing reaction conditions. Europium ions in YPO4:Eu and YVO4:Eu was successfully reduced to Eu2+ ions by sodium borohydride under reflux. The peak position of blue emission due to Eu2+ ions (4f-5d transition) in nanocrystals was different among the materials (Y2O3, YVO4 and YPO4).
Mitsunobu Iwasaki,Naoki Yamashita,Masato Taguchi,Subbian Karuppucharmy,Seishiro Ito, andWonkyu Park
"Blue emission of YMO4:Eu2+ (M=V,P) nanocrystals prepared through facile wet process", Proc. SPIE 6321, Nanophotonic Materials III, 632104 (11 September 2006); https://doi.org/10.1117/12.681097
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Mitsunobu Iwasaki, Naoki Yamashita, Masato Taguchi, Subbian Karuppucharmy, Seishiro Ito, Wonkyu Park, "Blue emission of YMO4:Eu2+ (M=V,P) nanocrystals prepared through facile wet process," Proc. SPIE 6321, Nanophotonic Materials III, 632104 (11 September 2006); https://doi.org/10.1117/12.681097