Ms. Zhangfan Jiang Profile

Zhangfan Jiang

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Proceedings Article | 22 March 2021 Presentation + Paper

Printability characterization of graphene-reinforced cementitious composites

Ugur Kilic, Zhangfan Jiang, Ji Ma, Osman Ozbulut

Proceedings Volume 11589, 1158904 (2021) https://doi.org/10.1117/12.2585595

KEYWORDS: Cements, Composites, Printing, 3D printing, Scanning electron microscopy, Nanomaterials, Additive manufacturing, Raman spectroscopy, Optical microscopy, Manufacturing

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The cement-based additive manufacturing, commonly known as 3D concrete printing, facilitates the use of advanced cementitious materials in construction as this construction technique minimizes waste and enables the optimal placement of the material. 3D printable cementitious mixtures should have specific consistency for successful manufacturing. In particular, they should be extruded smoothly during the printing process while maintain their shape after deposition, both of which are closely related to the rheological properties of cementitious mixture. The use of graphene in cementitious composites has been widely explored in recent years and it was shown that graphene can improve the mechanical properties and durability of cementitious composites. However, the rheological properties and printability characteristics of graphene-reinforced cementitious materials still remain underexplored. This study investigates the effects of graphene nanoplatelets (GNPs) on rheological and printability characteristics of GNP-reinforced cementitious composites. GNPs are added into cementitious mixtures, designed for 3D concrete printing applications, at concentration of 0%, 0.05%, 0.10%, 0.15%, 0.20%, and 0.25% by weight of cement. GNPs are first dispersed into water through the help of ultrasonic treatment and a polycarboxylate-based superplasticizer. The dispersion quality of GNPs is assessed through UV-vis absorption spectroscopy, optical microscopy, and Raman spectroscopy. Then, the rheological properties of GNP-reinforced mortar composites are studied using a shear rheometer via stress-growth tests, shear rate ramp up-down tests, and structural recovery tests.

Proceedings Article | 22 March 2021 Presentation + Paper

Mechanical properties and durability of cementitious composites reinforced by graphene nanoplatelets with different particle size and surface area

Zhangfan Jiang, Ugur Kilic, Osman Ozbulut

Proceedings Volume 11589, 115890E (2021) https://doi.org/10.1117/12.2584919

Read Abstract +

Despite being most widely used construction materials, cement-based composites are brittle materials with low tensile strength and susceptible to cracking, especially under harsh environments. Over the past three decades, numerous studies have been conducted to enhance the mechanical properties and durability of cementitious composites through the use of various nanomaterials such as carbon nanotubes (CNTs) and carbon nanofibers (CNFs). More recently, graphene nanoplatelets (GNPs) has emerged as an ideal 2D nano-reinforcement for composite materials due to their favorable mechanical, thermal and electrical properties. However, the effects of different dispersing agents and particle size and surface area of GNPs on the mechanical properties of cement-based composites needs to be further investigated. This paper explores the influence of GNP addition on the mechanical properties and durability of cement-based composites. Two types of GNPs with different lateral size (<2 μm and 25 μm) and specific surface area (300 m²/g and 120 m²/g) are used in this study. The GNP concentration is set to be 0.1% by weight of cement in all mixtures. In order to study the effect of dispersion agents, four different dispersion method are utilized to disperse and stabilize GNP particles in aqueous solution. Compressive strength and flexural strength tests are conducted to assess the mechanical properties, while sorptivity test and surface resistivity measurement are carried out to evaluate the durability. In order to explore the effect of GNPs on hydration process of cement mortar, mechanical properties tests are conducted at 7 day and 28 day curing ages and thermal gravimetric analyses are conducted.

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