The electrochemical properties of NiCo2O4 for using as electrode materials for the potential applications have been investigated by electrochemical measurement which composed of cyclic voltammetry (CV) and galvanostatic chargedischarge (GCD). These processes are generating the ion exchange between the electrode and electrolyte, wherein induce the surface change of the interface. Especially, since in the cycle ability measurement using the potentiostat needed to repeat the cycle into the electrode for many times, the effective of the electrode is reduced. In this research, digital holographic technique was used to investigate the different properties of interface of the NiCo2O4 electrode while operating under the various electrochemical techniques. In our DH recording, the surface change of the electrode was expose at the difference potential scan rate at 1, 5, 10, 50, 100 and 200 mV/s of CV, and the difference current densities at 1, 2, 3, 5, 10 and 20 A/g of GCD and vary times of cycle ability test every 50 cycle times to 1000 cycles. In the end the reconstructed DH images of the electrode have been used to analyze the results from electrochemical measurement.
In this paper we propose a modern technique to evaluate the shape changes of solder paste by using double-view in-line digital holography. We observed the transformation of three different kinds of solder paste composition: pure solder paste, solder paste mixed with 0.02%, 0.05%, 0.10% graphene (GPN) and 0.02%, 0.05%, 0.10% graphene oxide (GPNO), respectively. The shape of the solder pastes was investigated at different melt temperatures (i.e. 200°C, 250°C, and 300°C) for 30 seconds using a collimated beam propagating through the solder paste, then being double reflected on a mirror and second incident on another sides of the solder paste. The double images bearing beams were recorded with a CCD sensor simultaneously. The single recorded digital hologram from double view technique was reconstructed using digital holography. The results show that the double-view technique provides reliably data. Moreover, it would be developed for observing more than two images by single holography writing in the future.
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